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Beilstein J. Org. Chem. 2019, 15, 2922–2929, doi:10.3762/bjoc.15.286
Graphical Abstract
Figure 1: Chemical structures of naturally occurring argyrins with potent antipseudomonal activity.
Figure 2: The biosynthetic pathway for argyrin production in Cystobacter sp. SBCb004 (Arg1, radical SAM-depen...
Figure 3: Designed mutasynthons 9–14 for argyrin biosynthesis. Peptides are based on three amino acids and ad...
Scheme 1: Synthesis of tripeptide thioesters. Reagents and conditions: (a) SOCl2, EtOH, 78 °C; (b) IBCF, NMM,...
Scheme 2: Improved synthesis of the tripeptide thioester 14. Reagents and conditions: (a) SOCl2, EtOH, 78 °C;...
Figure 4: Analysis of mutasynthon 14 obtained via the convergent synthetic route by HPLC on a HILIC stationar...
Beilstein J. Org. Chem. 2016, 12, 2828–2833, doi:10.3762/bjoc.12.282
Figure 1: Alkylseleno glycosides, such as 1, are used as tools for X-ray crystallography of lectins. Some lec...
Scheme 1: Synthesis of 3 through initial introduction of the seleno aglycon and subsequent O-methylation. Rea...
Scheme 2: Synthesis of compound 3 via initial selective 2-O-methylation followed by the introduction of the s...